One Pot Procedure
한 냄비 절차

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In a one pot procedure a series of ( R )-2-((2 S ,3 S )-3-((1-(4-chlorophenyl)-1 H -1,2,3-triazol-4-yl)methoxy)-3,6-dihydro-2 H -pyran-2-yl)-3-phenylthiazolidin-4-ones 9a – g and 2-((2 R )-2-((2 S ,3 S )-3-((1-(4-chlorophenyl)-1 H -1,2,3-triazol-4-yl)methoxy)-3,6-dihydro-2 H -pyran-2-yl)-4-oxo-3-phenylthiazolidin-5-yl)acetic acids 10a – g was prepared by condensation of (2 S ,3 S )-3-((1-(4-chlorophenyl)-1 H -1,2,3-triazol-4-yl)methoxy)-3,6-dihydro-2 H -pyran-2-carbaldehyde with mercapto acids and primary amines in the presence of ZnCl 2 under both microwave irradiation and conventional heating conditions.

원 포트 절차에서 일련의 ( R )-2-((2S,3S)-3-((1-(4-클로로페닐)-1H-1,2,3-트리아졸-4-일) 메톡시)-3,6-디히드로-2H-피란-2-일)-3-페닐티아졸리딘-4-온 9a-g 및 2-((2R)-2-((2S,3S)-3 -((1-(4-클로로페닐)-1H-1,2,3-트리아졸-4-일)메톡시)-3,6-디히드로-2H-피란-2-일)-4-옥소-3 -페닐티아졸리딘-5-일)아세트산 10a-g는 (2S,3S)-3-((1-(4-클로로페닐)-1H-1,2,3-트리아졸-4-의 축합에 의해 제조됨 일)메톡시)-3,6-디하이드로-2H-피란-2-카브알데하이드와 메르캅토산 및 1차 아민을 마이크로파 조사 및 통상적인 가열 조건 하에 ZnCl2의 존재하에.

Microwave-assisted Synthesis and Anticancer Activity of Triazolyl Thiazolidine Derivatives of Pyrene

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10.1002/jlcr.3709

MPP-(CH2 )3 -N3 was synthesized via three efficient and reliable chemical synthesis steps (more than 80% yield) then radiolabeled by addition of 2-ethynylpyridine and [99m Tc][Tc(CO)3 (H2 O)3 ]+ precursor in one pot procedure (more than 95% radiochemical efficiency) through click chemistry method.

MPP-(CH2)3-N3는 3개의 효율적이고 신뢰할 수 있는 화학적 합성 단계(수율 80% 이상)를 통해 합성된 다음 2-에티닐피리딘 및 [99m Tc][Tc(CO)3(H2O)3]를 첨가하여 방사성 표지되었습니다. + Click chemistry 방법을 통한 one pot 절차(95% 이상의 방사화학적 효율)의 전구체.

New 99m Tc(CO)3 -radiolabeled arylpiperazine pharmacophore as potent 5HT1A serotonin receptor radiotracer: Docking studies, chemical synthesis, radiolabeling, and biological evaluation.

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10.1016/j.ejmech.2019.111586

In a one pot procedure, we discovered both the ring opening reaction of the three-membered ring and the cleavage of the sulfonamide protecting moiety at the same time.

원 포트 절차에서 우리는 3원 고리의 개환 반응과 설폰아미드 보호 부분의 절단을 동시에 발견했습니다.

Synthesis of novel tellurides bearing benzensulfonamide moiety as carbonic anhydrase inhibitors with antitumor activity.

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10.29356/JMCS.V53I3.993

The transfor- mation was produced under mild conditions providing high yields (70-87%), in a one pot procedure (some acetylated starting material is recovered).

변환은 원 포트 절차(일부 아세틸화된 출발 물질이 회수됨)로 높은 수율(70-87%)을 제공하는 온화한 조건에서 생성되었습니다.

Side-chain opening of steroidal sapogenins to form 22-oxocholestanic skeletons: An approach to analogues of the aglycone of the potent anticancer agent OSW-1

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One Pot Procedure 한 냄비 절차 - MPP-(CH2 )3 -N3 was synthesized via three efficient and reliable chemical synthesis steps (more than 80% yield) then radiolabeled by addition of 2-ethynylpyridine and [99m Tc][Tc(CO)3 (H2 O)3 ]+ precursor in one pot procedure (more than 95% radiochemical efficiency) through click chemistry method. [1] In a one pot procedure, we discovered both the ring opening reaction of the three-membered ring and the cleavage of the sulfonamide protecting moiety at the same time. [2] The transfor- mation was produced under mild conditions providing high yields (70-87%), in a one pot procedure (some acetylated starting material is recovered). [3]
MPP-(CH2)3-N3는 3개의 효율적이고 신뢰할 수 있는 화학적 합성 단계(수율 80% 이상)를 통해 합성된 다음 2-에티닐피리딘 및 [99m Tc][Tc(CO)3(H2O)3]를 첨가하여 방사성 표지되었습니다. + Click chemistry 방법을 통한 one pot 절차(95% 이상의 방사화학적 효율)의 전구체. [1] 원 포트 절차에서 우리는 3원 고리의 개환 반응과 설폰아미드 보호 부분의 절단을 동시에 발견했습니다. [2] 변환은 원 포트 절차(일부 아세틸화된 출발 물질이 회수됨)로 높은 수율(70-87%)을 제공하는 온화한 조건에서 생성되었습니다. [3]

3 1 4 3 1 4

In a one pot procedure a series of ( R )-2-((2 S ,3 S )-3-((1-(4-chlorophenyl)-1 H -1,2,3-triazol-4-yl)methoxy)-3,6-dihydro-2 H -pyran-2-yl)-3-phenylthiazolidin-4-ones 9a – g and 2-((2 R )-2-((2 S ,3 S )-3-((1-(4-chlorophenyl)-1 H -1,2,3-triazol-4-yl)methoxy)-3,6-dihydro-2 H -pyran-2-yl)-4-oxo-3-phenylthiazolidin-5-yl)acetic acids 10a – g was prepared by condensation of (2 S ,3 S )-3-((1-(4-chlorophenyl)-1 H -1,2,3-triazol-4-yl)methoxy)-3,6-dihydro-2 H -pyran-2-carbaldehyde with mercapto acids and primary amines in the presence of ZnCl 2 under both microwave irradiation and conventional heating conditions. [1]
원 포트 절차에서 일련의 ( R )-2-((2S,3S)-3-((1-(4-클로로페닐)-1H-1,2,3-트리아졸-4-일) 메톡시)-3,6-디히드로-2H-피란-2-일)-3-페닐티아졸리딘-4-온 9a-g 및 2-((2R)-2-((2S,3S)-3 -((1-(4-클로로페닐)-1H-1,2,3-트리아졸-4-일)메톡시)-3,6-디히드로-2H-피란-2-일)-4-옥소-3 -페닐티아졸리딘-5-일)아세트산 10a-g는 (2S,3S)-3-((1-(4-클로로페닐)-1H-1,2,3-트리아졸-4-의 축합에 의해 제조됨 일)메톡시)-3,6-디하이드로-2H-피란-2-카브알데하이드와 메르캅토산 및 1차 아민을 마이크로파 조사 및 통상적인 가열 조건 하에 ZnCl2의 존재하에. [1]